LabReport (#316)

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"# Certificate of Analysis\n\n## KCA Laboratories\n\n232 North Plaza Drive \nNicholasville, KY 40356 \n+1-833-KCA-LABS \nhttps:\/\/kcalabs.com \nKDA Lic.# P.0058 \n\n----\n\n### D9THCP-060724.1\n\n- **Sample ID:** SA-240610-420000 \n- **Batch:** D9THCP-060724.1 \n- **Type:** Raw Material \n- **Matrix:** Concentrate - Distillate \n- **Unit Mass (g):** \n\n**Received:** 06\/11\/2024 \n**Completed:** 06\/20\/2024 \n\n### Client\n\nMC Nutraceuticals \n6101 Long Prairie Rd, Ste 144 LB 17 \nFlower Mound, TX 75028 \nUSA \n\n----\n\n### Summary\n\n| Test | Date Tested | Status |\n|-------------------|-------------|--------|\n| Cannabinoids | 06\/18\/2024 | Tested |\n| Heavy Metals | 06\/20\/2024 | Tested |\n| Pesticides | 06\/20\/2024 | Tested |\n| Residual Solvents | 06\/20\/2024 | Tested |\n\n- **ND** Total \u03949-THC\n- **87.0%** \u03949-THCP\n- **87.7%** Total Cannabinoids\n- **Not Tested** Moisture Content\n- **Not Tested** Foreign Matter\n- **Yes** Internal Standard Normalization\n\n----\n\n### Cannabinoids by HPLC-PDA and GC-MS\/MS\n\n| Analyte | LOD (%) | LOQ (%) | Result (%) | Result (mg\/g) |\n|-----------|---------|---------|------------|---------------|\n| CBC | 0.004 | 0.012 | ND | ND |\n| CBCV | 0.004 | 0.012 | ND | ND |\n| CBD | 0.004 | 0.012 | ND | ND |\n| CBDV | 0.004 | 0.012 | ND | ND |\n| CBDV | 0.004 | 0.012 | ND | ND |\n| CBG | 0.004 | 0.012 | ND | ND |\n| CBL | 0.004 | 0.012 | ND | ND |\n| CBN | 0.004 | 0.012 | ND | ND |\n| CBT | 0.004 | 0.012 | ND | ND |\n| \u03948-THC | 0.010 | 0.031 | ND | ND |\n| \u03948-THCP | 0.010 | 0.031 | ND | ND |\n| \u03948-THCV | 0.010 | 0.031 | ND | ND |\n| \u03949-THC | 0.006 | 0.018 | ND | ND |\n| \u03949-THCP | 0.006 | 0.018 | 0.877 | 8.77 |\n| \u03949-THCV | 0.006 | 0.018 | ND | ND |\n\n**Total \u03949-THC Total**: ND\n\n----\n\n**ND** = Not Detected; **NT** = Not Tested; **LOD** = Limit of Detection; **LOQ** = Limit of Quantitation; **RL** = Reporting Limit; \u0394 = Delta; Total \u03949-THC = \u03949-THCA * 0.877 + \u03949-THC; Total CBD = CBDA * 0.877 + CBD.\n\n----\n\nGenerated By: Alex Morris \nQuality Manager \nDate: 06\/20\/2024 \n\nTested By: Nicholas Howard \nScientist \nDate: 06\/18\/2024 \n\nThis product or substance has been tested by KCA Laboratories using validated testing methodologies and an ISO\/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substance tested. The report relates to the sample analyzed only in the state received. Results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCA Laboratories assumes no responsibility to anyone other than the client with respect to the test results, and will only be liable for proven negligence. KCA Laboratories makes no claims regarding the status of this product under any federal, state, or local law. This Certificate of Analysis shall not be reproduced except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.\n---\n# Certificate of Analysis\n\n## KCA Laboratories\n\n232 North Plaza Drive \nNicholasville, KY 40356 \n+1-833-KCA-LABS \nhttps:\/\/kcalabs.com \nKDA Lic.# P.0058 \n\n----\n\n### D9THCP-060724.1\n\n- **Sample ID:** SA-246010-420000 \n- **Batch:** D9THCP-060724.1 \n- **Type:** Raw Material \n- **Matrix:** Concentrate - Distillate \n- **Unit Mass (g):** \n\n**Received:** 06\/11\/2024 \n**Completed:** 06\/20\/2024 \n\n### Client\n\nMC Nutraceuticals \n6101 Long Prairie Rd, Ste 144 LB 17 \nFlower Mound, TX 75028 \nUSA \n\n----\n\n## Heavy Metals by ICP-MS\n\n| Analyte | LOD (ppm) | LOQ (ppm) | Result (ppm) |\n|-----------|-----------|-----------|--------------|\n| Arsenic | 0.002 | 0.02 | ND |\n| Cadmium | 0.001 | 0.02 | ND |\n| Lead | 0.002 | 0.02 | ND |\n| Mercury | 0.012 | 0.05 | ND |\n\nND = Not Detected; NT = Not Tested; LOD = Limit of Detection; LOQ = Limit of Quantitation; P = Pass; F = Fail; RL = Reporting Limit; Values over action limits may be estimates\n\n----\n\nGenerated By: Alex Morris \nQuality Manager \nDate: 06\/20\/2024 \n\nTested By: Chris Farnan \nScientist \nDate: 06\/20\/2024 \n\nThis product or substance has been tested by KCA Laboratories using validated testing methodologies in an ISO\/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substance tested. The reported result is based on a sample weight. Unless otherwise stated, results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCA Laboratories makes no claims as to the efficacy, safety or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certificate of Analysis shall not be reproduced except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.\n---\n# Certificate of Analysis\n\n**KCA Laboratories** \n232 North Plaza Drive \nNicholasville, KY 40356 \n+1-833-KCA-LABS \nhttps:\/\/kcalabs.com \nKDA Lic.# P_0058 \n\n----\n\n**Sample ID:** SA-246010-42000 \n**Batch:** D9THCP-060724.1 \n**Type:** Raw Material \n**Matrix:** Concentrate - Distillate \n**Unit Mass (g):** \n\n**Received:** 06\/11\/2024 \n**Completed:** 06\/20\/2024 \n\n**Client** \nMC Nutraceuticals \n6101 Long Prairie Rd, Ste 144 LB 17 \nFlower Mound, TX 75028 \nUSA \n\n----\n\n## Pesticides by LC-MS\/MS\n\n| Analyte | LOD (ppb) | LOQ (ppb) | Result (ppb) |\n|-----------------------|-----------|-----------|--------------|\n| Abamectin | 30 | 100 | ND |\n| Acephate | 30 | 100 | ND |\n| Acetamiprid | 30 | 100 | ND |\n| Aldicarb | 30 | 100 | ND |\n| Azoxystrobin | 30 | 100 | ND |\n| Bifenazate | 30 | 100 | ND |\n| Bifenthrin | 30 | 100 | ND |\n| Boscalid | 30 | 100 | ND |\n| Carbaryl | 30 | 100 | ND |\n| Carbofuran | 30 | 100 | ND |\n| Chlorantraniliprole | 30 | 100 | ND |\n| Chlorpyrifos | 30 | 100 | ND |\n| Clofentezine | 30 | 100 | ND |\n| Coumaphos | 30 | 100 | ND |\n| Cypermethrin | 30 | 100 | ND |\n| Daminozide | 30 | 100 | ND |\n| Diazinon | 30 | 100 | ND |\n| Dichlorvos | 30 | 100 | ND |\n| Dimethoate | 30 | 100 | ND |\n| Dimethomorph | 30 | 100 | ND |\n| Ethoprophos | 30 | 100 | ND |\n| Etofenprox | 30 | 100 | ND |\n| Etoxazole | 30 | 100 | ND |\n| Fenhexamid | 30 | 100 | ND |\n| Fenoxycarb | 30 | 100 | ND |\n| Fenpyroximate | 30 | 100 | ND |\n| Fipronil | 30 | 100 | ND |\n| Flonicamid | 30 | 100 | ND |\n| Fludioxonil | 30 | 100 | ND |\n| Hexythiazox | 30 | 100 | ND |\n| Imazalil | 30 | 100 | ND |\n| Imidacloprid | 30 | 100 | ND |\n| Kresoxim methyl | 30 | 100 | ND |\n| Malathion | 30 | 100 | ND |\n| Metalaxyl | 30 | 100 | ND |\n| Methiocarb | 30 | 100 | ND |\n| Methomyl | 30 | 100 | ND |\n| Mevinphos | 30 | 100 | ND |\n| Myclobutanil | 30 | 100 | ND |\n| Naled | 30 | 100 | ND |\n| Oxamyl | 30 | 100 | ND |\n| Paclobutrazol | 30 | 100 | ND |\n| Permethrin | 30 | 100 | ND |\n| Phosmet | 30 | 100 | ND |\n| Piperonyl Butoxide | 30 | 100 | ND |\n| Prallethrin | 30 | 100 | ND |\n| Propiconazole | 30 | 100 | ND |\n| Pyproxyfen | 30 | 100 | ND |\n| Pyrethrins | 30 | 100 | ND |\n| Pyridaben | 30 | 100 | ND |\n| Spinetoram | 30 | 100 | ND |\n| Spinosad | 30 | 100 | ND |\n| Spiromesifen | 30 | 100 | ND |\n| Spirotetramat | 30 | 100 | ND |\n| Spiroxamine | 30 | 100 | ND |\n| Tebuconazole | 30 | 100 | ND |\n| Thiacloprid | 30 | 100 | ND |\n| Thiamethoxam | 30 | 100 | ND |\n| Trifloxystrobin | 30 | 100 | ND |\n\n**ND:** Not Detected; **NT:** Not Tested; **LOD:** Limit of Detection; **LOQ:** Limit of Quantitation; **P:** Pass; **F:** Fail; **RL:** Reporting Limit; Values over action limits may be estimates.\n\n----\n\n**Generated By:** Alex Morris \n**Quality Manager** \n**Date:** 06\/20\/2024 \n\n**Tested By:** Anthony Mattingly \n**Scientist** \n**Date:** 06\/20\/2024 \n\nThis product has been tested by KCA Laboratories using validated testing methodologies and an ISO\/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substance tested. The reported result is based on a sample weight. Unless otherwise stated, results are reported on an \"as received\" basis, without correction for moisture content. This Certificate of Analysis shall not be reproduced except in full, without the written approval of KCA Laboratories. KCA Laboratories makes no claims as to the efficacy, safety, or other uses associated with any detected or non-detected amounts of any substances reported herein.\n---\n# Certificate of Analysis\n\n## KCA Laboratories\n232 North Plaza Drive \nNicholasville, KY 40356 \n+1-833-KCA-LABS \nhttps:\/\/kcalabs.com \nKDA Lic.# P.0058 \n\n----\n\n### Sample Information\n- **Sample ID:** SA-246010-42000\n- **Batch:** D9THCP-060724.1\n- **Type:** Raw Material\n- **Matrix:** Concentrate - Distillate\n\n### Client\n- **Name:** MC Nutraceuticals\n- **Address:** 6101 Long Prairie Rd, Ste 144 LB 17 \n Flower Mound, TX 75028 \n USA\n\n### Dates\n- **Received:** 06\/11\/2024\n- **Completed:** 06\/20\/2024\n\n----\n\n## Residual Solvents by HS-GC-MS\n\n| Analyte | LOD (ppm) | LOQ (ppm) | Result (ppm) | Analyte | LOD (ppm) | LOQ (ppm) | Result (ppm) |\n|--------------------------|-----------|-----------|--------------|--------------------------|-----------|-----------|--------------|\n| Acetone | 167 | 500 | ND | Ethylene Oxide | 0.5 | 5 | ND |\n| Acetonitrile | 14 | 41 | ND | Heptane | 167 | 500 | ND |\n| Benzene | 0.5 | 1.5 | ND | n-Hexane | 167 | 500 | ND |\n| Butane | 50 | 150 | ND | Isobutane | 50 | 150 | ND |\n| 1-Butanol | 167 | 500 | ND | Isopropyl Acetate | 167 | 500 | ND |\n| 2-Butanol | 167 | 500 | ND | Isopropyl Alcohol | 167 | 500 | ND |\n| 2-Butanone | 167 | 500 | ND | Isopropylbenzene | 3 | 9 | ND |\n| Chloroform | 30 | 88 | ND | Methanol | 167 | 500 | ND |\n| Cyclohexane | 129 | 388 | ND | 2-Methylbutane | 50 | 150 | ND |\n| 1,2-Dichloroethane | 1 | 3 | ND | Methylene Chloride | 30 | 88 | ND |\n| 1,2-Dimethoxyethane | 4 | 10 | ND | 2-Methylpentane | 50 | 150 | ND |\n| Dimethyl Sulfoxide | 167 | 500 | ND | 3-Methylpentane | 50 | 150 | ND |\n| N,N-Dimethylacetamide | 30 | 88 | ND | n-Pentane | 50 | 150 | ND |\n| 2,2-Dimethylbutane | 10 | 29 | ND | 1-Pentanol | 167 | 500 | ND |\n| 3,3-Dimethylbutane | 10 | 29 | ND | n-Propanol | 167 | 500 | ND |\n| N,N-Dimethylformamide | 30 | 88 | ND | 1-Propanol | 167 | 500 | ND |\n| 2,2-Dimethylpropane | 167 | 500 | ND | Pyridine | 3 | 9 | ND |\n| 1,4-Dioxane | 1 | 3 | ND | Tetrahydrofuran | 30 | 88 | ND |\n| Ethanol | 167 | 500 | ND | Toluene | 30 | 88 | ND |\n| 2-Ethoxyethanol | 167 | 500 | ND | Trichloroethylene | 30 | 88 | ND |\n| Ethyl Acetate | 167 | 500 | ND | Xylenes (o-, m-, and p-) | 73 | 217 | ND |\n| Ethyl Ether | 167 | 500 | ND | | | | |\n| Ethylbenzene | 3 | 7 | ND | | | | |\n\n**ND = Not Detected; NT = Not Tested; LOD = Limit of Detection; LOQ = Limit of Quantitation; P = Pass; F = Fail; RL = Reporting Limit; Values over action limits may be estimates**\n\n----\n\n### Signatures\n\n- **Generated By:** Alex Morris \n **Quality Manager** \n **Date:** 06\/20\/2024\n\n- **Tested By:** Kelsey Rogers \n **Scientist** \n **Date:** 06\/20\/2024\n\n----\n\nThis product or substance has been tested by KCA Laboratories using validated testing methodologies in an ISO\/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substance tested. The reported result is based on a single analysis. Unless otherwise stated, results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCA Laboratories makes no claims to the efficacy, safety, or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certificate of Analysis shall not be reproduced except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.\n---\n# Certificate of Analysis\n\n## KCA Laboratories\n232 North Plaza Drive \nNicholasville, KY 40356 \n+1-833-KCA-LABS \nhttps:\/\/kcalabs.com \nKDA Lic.# P.0058 \n\n----\n\n### HHC-042424.1\n\n- **Sample ID:** SA-240425-39248\n- **Batch:** HHC-042424.1\n- **Type:** In-Process Material\n- **Matrix:** Concentrate - Distillate\n- **Unit Mass (g):** \n\n### Client\n- **Name:** MC Nutraceuticals\n- **Address:** 6101 Long Prairie Rd, Ste 144 LB 17 \n Flower Mound, TX 75028 \n USA\n\n----\n\n### Summary\n\n- **Test:** Cannabinoids\n- **Date Tested:** 05\/10\/2024\n- **Status:** Tested\n\n| ND | 62.3% | 92.8% | Not Tested | Not Tested | Yes |\n|----|-------|-------|------------|------------|-----|\n| Total \u03949-THC | (6aR,9R,10aR)-HHC | Total Cannabinoids | Moisture Content | Foreign Matter | Internal Standard Normalization |\n\n----\n\n### Cannabinoids by GC-MS\/MS\n\n| Analyte | LOD (%) | LOQ (%) | Result (%) | Result (mg\/g) |\n|-----------------------|---------|---------|------------|---------------|\n| CBC | 0.0095 | 0.0284 | ND | ND |\n| CBCV | 0.0128 | 0.0384 | ND | ND |\n| CBD | 0.0072 | 0.0216 | ND | ND |\n| CBDV | 0.0072 | 0.0216 | ND | ND |\n| CBG | 0.0177 | 0.0531 | ND | ND |\n| CBL | 0.0064 | 0.0192 | ND | ND |\n| CBN | 0.0064 | 0.0192 | 0.640 | 6.40 |\n| CBT | 0.0064 | 0.0192 | ND | ND |\n| \u03948-iso-THC | 0.0067 | 0.0202 | ND | ND |\n| \u03948-iso-THC | 0.0067 | 0.0202 | ND | ND |\n| \u03948-THC | 0.0067 | 0.0202 | ND | ND |\n| \u03949-THC | 0.0067 | 0.0202 | ND | ND |\n| \u03949-THCV | 0.0067 | 0.0202 | ND | ND |\n| (6aR,9R,10aR)-HHC | 0.0067 | 0.0202 | 62.3 | 623 |\n| (6aR,9S,10aR)-HHC | 0.0067 | 0.0202 | 30.4 | 304 |\n| Total | | | 92.8 | 928 |\n\n- **ND:** Not Detected\n- **NT:** Not Tested\n- **LOD:** Limit of Detection\n- **LOQ:** Limit of Quantitation\n- **R.L.:** Reporting Limit\n- **\u0394:** Delta\n- **Total \u03949-THC = \u03949-THC + \u03948-THC + \u03949-THCV**\n- **Total CBD = CBDA + CBD**\n- **Total CBG = CBGA + CBG**\n\n----\n\nGenerated By: Ryan Bellone \nCEO \nDate: 05\/10\/2024 \n\nTested By: Scott Caudill \nLaboratory Manager \nDate: 05\/10\/2024 \n\nThis product or substance has been tested by KCA Laboratories using validated testing methodologies and an ISO\/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substance tested. The report must not be used to imply certification or endorsement with any standard, test, or performance and quality of any similar material or article not tested or for acceptances established by KCA Laboratories. KCA Laboratories shall not be liable to the efficacy, safety, or other characteristics related to any tested or non-detected amounts of any substances reported herein. This Certificate of Analysis shall not be reproduced except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request."