LabReport (#322)

Null

"# 3Chi True Strains Gummy - Nirvana\n\n**Sample ID:** SA-231130-31023 \n**Batch:** 3ONOV23-TS-N1VGM \n**Type:** Finished Product - Ingestible \n**Matrix:** Edible - Gummy \n**Unit Mass (g):** 4.53063 \n\n**Received:** 12\/01\/2023 \n**Completed:** 12\/15\/2023 \n\n## Client\n**3Chi** \n275 Medical Dr #857 \nCarmel, IN 46082 \nUSA \nLic. #: 18_0235 \n\n## Summary\n\n| Test | Date Tested | Status |\n|-----------------|-------------|--------|\n| Cannabinoids | 12\/15\/2023 | Tested |\n| Heavy Metals | 12\/10\/2023 | Tested |\n| Microbials | 12\/06\/2023 | Tested |\n| Mycotoxins | 12\/07\/2023 | Tested |\n| Pesticides | 12\/07\/2023 | Tested |\n| Residual Solvents | 12\/08\/2023 | Tested |\n\n| ND | 1.76% | 2.33% | Not Tested | Not Tested | Yes |\n|----------------|-------------|-------------|--------------|--------------|----------------------|\n| Total \u03949-THC | \u03948-THC | Total Cannabinoids | Moisture Content | Foreign Matter | Internal Standard Normalization |\n\n## Cannabinoids by HPLC-PDA and\/or GC-MS\/MS\n\n| Analyte | LOD (%) | LOQ (%) | Result (%) | Result (mg\/unit) |\n|-----------------|---------|---------|------------|------------------|\n| CBC | 0.0018 | 0.0054 | ND | ND |\n| CBCA | 0.0018 | 0.0054 | ND | ND |\n| CBCV | 0.0018 | 0.0054 | ND | ND |\n| CBD | 0.0018 | 0.0054 | ND | ND |\n| CBDA | 0.0018 | 0.0054 | ND | ND |\n| CBDV | 0.0018 | 0.0054 | ND | ND |\n| CBE | 0.0018 | 0.0054 | ND | ND |\n| CBG | 0.0018 | 0.0054 | 0.0282 | 1.28 |\n| CBGA | 0.0018 | 0.0054 | ND | ND |\n| CBL | 0.0018 | 0.0054 | ND | ND |\n| CBLA | 0.0018 | 0.0054 | ND | ND |\n| CBN | 0.0018 | 0.0054 | 0.00438 | 0.20 |\n| CBNA | 0.0018 | 0.0054 | ND | ND |\n| CBT | 0.0018 | 0.0054 | ND | ND |\n| \u03944,8-iso-THC | 0.0020 | 0.0061 | ND | ND |\n| \u03948-iso-THC | 0.0020 | 0.0061 | ND | ND |\n| \u03948-THC | 0.0020 | 0.0061 | 1.76 | 79.8 |\n| \u03948-THCV | 0.0020 | 0.0061 | 0.034 | 1.54 |\n| \u03949-THC | 0.0020 | 0.0061 | ND | ND |\n| \u03949-THCA | 0.0020 | 0.0061 | ND | ND |\n| \u03949-THCV | 0.0020 | 0.0061 | ND | ND |\n| \u03949-THCVA | 0.0020 | 0.0061 | ND | ND |\n| \u03949-THCP | 0.0020 | 0.0061 | ND | ND |\n| exo-THC | 0.0020 | 0.0061 | ND | ND |\n| (6aR,9R,10aR)-HHC | 0.0067 | 0.0202 | 0.142 | 6.43 |\n| (6aR,9S,10aR)-HHC | 0.0067 | 0.0202 | 0.00448 | 0.20 |\n\n**Total \u03949-THC:** ND \n**Total:** 2.33% \n**Total (mg\/unit):** 106 \n\n----\n\n**Generated By:** Ryan Bellone \n**CCO** \n**Date:** 12\/15\/2023 \n\n**Tested By:** Scott Caudill \n**Laboratory Manager** \n**Date:** 12\/15\/2023 \n\nThis product or substance has been tested by KCA Laboratories using validated testing methodologies in an ISO\/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substance tested. The reported result is based on a single weight. Unless otherwise stated, results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCA Laboratories makes no claims as to the efficacy, safety, or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certificate of Analysis shall not be reproduced except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.\n---\n# 3Chi True Strains Gummy - Nirvana\n\n**Sample ID:** SA-231130-31023 \n**Batch:** 3NOV23-TS-NIRVM \n**Type:** Finished Product - Ingestible \n**Matrix:** Edible - Gummy \n**Unit Mass (g):** 4.53063 \n\n**Client** \n3Chi \n275 Medical Dr #857 \nCarmel, IN 46082 \nUSA \nLic. #: 18_0235 \n\n**Received:** 12\/01\/2023 \n**Completed:** 12\/15\/2023 \n\n## Heavy Metals by ICP-MS\n\n| Analyte | LOD (ppb) | LOQ (ppb) | Result (ppb) |\n|-----------|-----------|-----------|--------------|\n| Arsenic | 2 | 20 | ND |\n| Cadmium | 1 | 20 | ND |\n| Lead | 2 | 20 | <LOQ |\n| Mercury | 1 | 50 | ND |\n\nND = Not Detected \nNT = Not Tested \nLOD = Limit of Detection \nLOQ = Limit of Quantitation \nP = Pass \nF = Fail \nRL = Reporting Limit \n\n----\n\n**Generated By:** Ryan Bellone \n**CCO** \n**Date:** 12\/15\/2023 \n\n**Tested By:** Kelsey Rogers \n**Scientist** \n**Date:** 12\/12\/2023 \n\nThis product or substance has been tested by KCA Laboratories using validated testing methodologies in an ISO\/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substance tested. The reported result is based on a sample weight. Unless otherwise stated, results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCA Laboratories makes no claims as to the efficacy, safety, or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certificate of Analysis shall not be reproduced except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.\n---\n# 3Chi True Strains Gummy - Nirvana\n\n**Sample ID:** SA-231130-31023 \n**Batch:** 3NOV23-TS-NIRVM \n**Type:** Finished Product - Ingestible \n**Matrix:** Edible - Gummy \n**Unit Mass (g):** 4.53063 \n\n**Received:** 12\/01\/2023 \n**Completed:** 12\/15\/2023 \n\n**Client** \n3Chi \n275 Medical Dr #857 \nCarmel, IN 46082 \nUSA \nLic. #: 18_0235 \n\n## Pesticides by LC-MS\/MS\n\n| Analyte | LOD (ppb) | LOQ (ppb) | Result (ppb) | Analyte | LOD (ppb) | LOQ (ppb) | Result (ppb) |\n|-----------------------|-----------|-----------|--------------|-----------------------|-----------|-----------|--------------|\n| Acephate | 30 | 100 | ND | Hexythiazox | 30 | 100 | ND |\n| Acetamiprid | 30 | 100 | ND | Imazalil | 30 | 100 | ND |\n| Aldicarb | 30 | 100 | ND | Imidacloprid | 30 | 100 | ND |\n| Azoxystrobin | 30 | 100 | ND | Kresoxim methyl | 30 | 100 | ND |\n| Bifenazate | 30 | 100 | ND | Malathion | 30 | 100 | ND |\n| Bifenthrin | 30 | 100 | ND | Metalaxyl | 30 | 100 | ND |\n| Boscalid | 30 | 100 | ND | Methiocarb | 30 | 100 | ND |\n| Carbaryl | 30 | 100 | ND | Methomyl | 30 | 100 | ND |\n| Carbofuran | 30 | 100 | ND | Mevinphos | 30 | 100 | ND |\n| Chlorantraniliprole | 30 | 100 | ND | Myclobutanil | 30 | 100 | ND |\n| Chlorpyrifos | 30 | 100 | ND | Naled | 30 | 100 | ND |\n| Clofentezine | 30 | 100 | ND | Oxamyl | 30 | 100 | ND |\n| Clopyralid | 30 | 100 | ND | Paclobutrazol | 30 | 100 | ND |\n| Cyfluthrin | 30 | 100 | ND | Permethrin | 30 | 100 | ND |\n| Cypermethrin | 30 | 100 | ND | Phosmet | 30 | 100 | ND |\n| Daminozide | 30 | 100 | ND | Piperonyl Butoxide | 30 | 100 | ND |\n| Diazinon | 30 | 100 | ND | Prallethrin | 30 | 100 | ND |\n| Dichlorvos | 30 | 100 | ND | Propiconazole | 30 | 100 | ND |\n| Dimethoate | 30 | 100 | ND | Pyrethrins | 30 | 100 | ND |\n| Dimethomorph | 30 | 100 | ND | Pyridaben | 30 | 100 | ND |\n| Ethoprophos | 30 | 100 | ND | Spinetoram | 30 | 100 | ND |\n| Etofenprox | 30 | 100 | ND | Spinosad | 30 | 100 | ND |\n| Etoxazole | 30 | 100 | ND | Spiromesifen | 30 | 100 | ND |\n| Fenhexamid | 30 | 100 | ND | Spirotetramat | 30 | 100 | ND |\n| Fenoxycarb | 30 | 100 | ND | Spiroxamine | 30 | 100 | ND |\n| Fenpyroximate | 30 | 100 | ND | Tebuconazole | 30 | 100 | ND |\n| Fipronil | 30 | 100 | ND | Thiacloprid | 30 | 100 | ND |\n| Flonicamid | 30 | 100 | ND | Thiamethoxam | 30 | 100 | ND |\n| Fludioxonil | 30 | 100 | ND | Trifloxystrobin | 30 | 100 | ND |\n\n**ND = Not Detected** \n**NT = Not Tested** \n**LOD = Limit of Detection** \n**LOQ = Limit of Quantitation** \n**P = Pass** \n**F = Fail** \n**RL = Reporting Limit**\n\n----\n\n**Generated By:** Ryan Bellone \n**CCO** \n**Date:** 12\/15\/2023 \n\n**Tested By:** Jasper van Heemst \n**Principal Scientist** \n**Date:** 12\/07\/2023 \n\nThis product or substance has been tested by KCA Laboratories using validated testing methodologies in an ISO\/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substance tested. The reported result is based on a sample weight. Unless otherwise stated, results of tests performed on all quality control samples criteria for acceptance established by KCA Laboratories. KCA Laboratories makes no claims as to the efficacy, safety or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certificate of Analysis shall not be reproduced except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.\n---\n# 3Chi True Strains Gummy - Nirvana\n\n**Sample ID:** SA-231130-31023 \n**Batch:** 3NOV23-TS-N1VGM \n**Type:** Finished Product - Ingestible \n**Matrix:** Edible - Gummy \n**Unit Mass (g):** 4.53063 \n\n**Received:** 12\/01\/2023 \n**Completed:** 12\/15\/2023 \n\n**Client** \n3Chi \n275 Medical Dr #857 \nCarmel, IN 46082 \nUSA \nLic. #: 18_0235 \n\n## Mycotoxins by LC-MS\/MS\n\n| Analyte | LOD (ppb) | LOQ (ppb) | Result (ppb) |\n|---------------|-----------|-----------|--------------|\n| B1 | 1 | 5 | ND |\n| B2 | 1 | 5 | ND |\n| G1 | 1 | 5 | ND |\n| G2 | 1 | 5 | ND |\n| Ochratoxin A | 1 | 5 | ND |\n\nND = Not Detected; NT = Not Tested; LOD = Limit of Detection; LOQ = Limit of Quantitation; P = Pass; F = Fail; RL = Reporting Limit\n\n----\n\n**Generated By:** Ryan Bellone \n**Date:** 12\/15\/2023 \n\n**Tested By:** Jasper van Heemst \n**Principal Scientist** \n**Date:** 12\/07\/2023 \n\nThis product or substance has been tested by KCA Laboratories using validated testing methodologies in an ISO\/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substance tested. The reported result is based on a sample weight. Unless otherwise stated, results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCA Laboratories makes no claims as to the efficacy, safety, or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certificate of Analysis shall not be reproduced except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.\n---\n# 3Chi True Strains Gummy - Nirvana\n\n**Sample ID:** SA-231130-31023 \n**Batch:** 3ONOV23-TS-N1VGM \n**Type:** Finished Product - Ingestible \n**Matrix:** Edible - Gummy \n**Unit Mass (g):** 4.53063 \n\n**Received:** 12\/01\/2023 \n**Completed:** 12\/15\/2023 \n\n**Client** \n3Chi \n275 Medical Dr #857 \nCarmel, IN 46082 \nUSA \nLic. #: 18_0235 \n\n## Microbials by PCR and Plating\n\n| Analyte | LOD (CFU\/g) | Result (CFU\/g) | Result (Qualitative) |\n|--------------------------------------|-------------|----------------|----------------------------|\n| Total aerobic count | 10 | ND | |\n| Total coliforms | 10 | ND | |\n| Generic E. coli | 1 | ND | |\n| Salmonella spp. | 1 | | Not Detected per 1 gram |\n| Shiga-toxin producing E. coli (STEC) | 1 | | Not Detected per 1 gram |\n\nND = Not Detected; NT = Not Tested; LOD = Limit of Detection; LOQ = Limit of Quantitation; CFU = Colony Forming Units; P = Pass; F = Fail; R.L. = Reporting Limit\n\n----\n\n**Generated By:** Ryan Bellone \n**CCO** \n**Date:** 12\/15\/2023 \n\n**Tested By:** Matt Zachman \n**Laboratory Technician** \n**Date:** 12\/06\/2023 \n\nThis product or substance has been tested by KCA Laboratories using validated testing methodologies in an ISO\/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substance tested. The reported result is based on a sample weight. Unless otherwise stated, results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCA Laboratories makes no claims as to the efficacy, safety or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certificate of Analysis shall not be reproduced except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.\n---\n# 3Chi True Strains Gummy - Nirvana\n\n**Sample ID:** SA-231130-31023 \n**Batch:** 3ONOV23-TS-NIRVM \n**Type:** Finished Product - Ingestible \n**Matrix:** Edible - Gummy \n**Unit Mass (g):** 4.53063 \n\n**Received:** 12\/01\/2023 \n**Completed:** 12\/15\/2023 \n\n**Client** \n3Chi \n275 Medical Dr #857 \nCarmel, IN 46082 \nUSA \nLic. #: 18_0235 \n\n## Residual Solvents by HS-GC-MS\n\n| Analyte | LOD (ppm) | LOQ (ppm) | Result (ppm) |\n|-----------------------------|-----------|-----------|--------------|\n| Acetone | 167 | 500 | ND |\n| Acetonitrile | 14 | 50 | ND |\n| Benzene | 0.5 | 1.5 | ND |\n| Butane | 167 | 500 | ND |\n| 1-Butanol | 167 | 500 | ND |\n| 2-Butanol | 167 | 500 | ND |\n| Chloroform | 5 | 16 | ND |\n| Cyclohexane | 129 | 388 | ND |\n| 1,2-Dichloroethane | 1 | 3 | ND |\n| 1,1-Dimethoxyethane | 10 | 29 | ND |\n| Dimethyl Sulfoxide | 167 | 500 | ND |\n| 2,3-Dimethylbutane | 10 | 29 | ND |\n| 2,2-Dimethylbutane | 10 | 29 | ND |\n| 2,2-Dimethylpropane | 10 | 29 | ND |\n| N,N-Dimethylformamide | 30 | 88 | ND |\n| 2,2-Dimethylpropane | 10 | 29 | ND |\n| 1,4-Dioxane | 13 | 30 | ND |\n| Ethanol | 167 | 500 | ND |\n| 2-Ethoxyethanol | 167 | 500 | ND |\n| Ethyl Acetate | 167 | 500 | ND |\n| Ethyl Ether | 3 | 10 | ND |\n| Ethylbenzene | 3 | 7 | ND |\n| Ethylene Oxide | 0.5 | 1 | ND |\n| Heptane | 167 | 500 | ND |\n| n-Hexane | 167 | 500 | ND |\n| Isobutane | 167 | 500 | ND |\n| Isopropyl Acetate | 167 | 500 | ND |\n| Isopropyl Alcohol | 167 | 500 | ND |\n| Isopropylbenzene | 167 | 500 | ND |\n| Methanol | 167 | 500 | ND |\n| 2-Methylbutane | 10 | 29 | ND |\n| Methylene Chloride | 1 | 3 | ND |\n| 2-Methylpentane | 10 | 29 | ND |\n| 3-Methylpentane | 10 | 29 | ND |\n| n-Pentane | 167 | 500 | ND |\n| 1-Pentanol | 167 | 500 | ND |\n| n-Propanol | 167 | 500 | ND |\n| 1-Propanol | 167 | 500 | ND |\n| Pyridine | 3 | 10 | ND |\n| Tetrahydrofuran | 30 | 89 | ND |\n| Toluene | 30 | 89 | ND |\n| Trichloroethylene | 3 | 10 | ND |\n| Xylenes (o-, m-, and p-) | 73 | 217 | ND |\n\n**ND = Not Detected; NT = Not Tested; LOD = Limit of Detection; LOQ = Limit of Quantitation; P = Pass; F = Fail; RL = Reporting Limit.**\n\n----\n\n**Generated By:** Ryan Bellone \n**Date:** 12\/15\/2023 \n\n**Tested By:** Scott Caudill \n**Laboratory Manager** \n**Date:** 12\/08\/2023 \n\nThis product or substance has been tested by KCA Laboratories using validated testing methodologies on an ISO\/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substance tested. The reported result is based on a sample weight. Unless otherwise stated, results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCA Laboratories makes no claims as to the efficacy, safety, or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certificate of Analysis shall not be reproduced except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request.\n---\n# 3Chi True Strains Gummy - Nirvana\n\n**Sample ID:** SA-231130-31023 \n**Batch:** 3ONOV23-TS-NIRVM \n**Type:** Finished Product - Ingestible \n**Matrix:** Edible - Gummy \n**Unit Mass (g):** 4.53063 \n\n**Received:** 12\/01\/2023 \n**Completed:** 12\/15\/2023 \n\n**Client** \n3Chi \n275 Medical Dr #857 \nCarmel, IN 46082 \nUSA \nLic. #: 18_0235 \n\n----\n\n## Reporting Limit Appendix\n\n### Heavy Metals - Colorado CDPHE\n\n| Analyte | Limit (ppb) |\n|----------|-------------|\n| Arsenic | 500 |\n| Cadmium | 500 |\n| Lead | 500 |\n| Mercury | 1500 |\n\n### Microbials\n\n| Analyte | Limit (CFU\/g) | Limit (CFU\/total g) |\n|---------|---------------|---------------------|\n| Total Yeast & Mold | 100 | - |\n| Total Aerobic Count | 1000 | - |\n\n### Residual Solvents - USP 467\n\n| Analyte | Limit (ppm) | Analyte | Limit (ppm) |\n|----------------------|-------------|----------------------|-------------|\n| Acetone | 5000 | Heptane | 5000 |\n| Acetonitrile | 410 | n-Hexane | 290 |\n| Benzene | 2 | Isopropyl Alcohol | 5000 |\n| Butane | 5000 | Isopropyl Acetate | 5000 |\n| 1-Butanol | 5000 | Methanol | 3000 |\n| 2-Butanol | 5000 | Methyl Isobutyl Ketone | 5000 |\n| Chloroform | 60 | Methylene Chloride | 600 |\n| Cyclohexane | 3880 | Pentane | 5000 |\n| 1,2-Dichloroethane | 5 | 2-Methylpentane | 5000 |\n| 1,1-Dichloroethene | 8 | 3-Methylpentane | 5000 |\n| Dimethyl Sulfoxide | 5000 | n-Pentanol | 5000 |\n| N,N-Dimethylacetamide| 1090 | n-Propane | 5000 |\n| 2,2-Dimethylbutane | 5000 | Propanol | 5000 |\n| 2,3-Dimethylbutane | 290 | Tetrahydrofuran | 720 |\n| N,N-Dimethylformamide| 880 | Toluene | 890 |\n| 2,2-Dimethylpropane | 5000 | Trichloroethylene | 80 |\n| 1,4-Dioxane | 380 | Xylenes (o-, m-, and p-) | 2170 |\n| Ethanol | 5000 | | |\n| 2-Ethoxyethanol | 160 | | |\n| Ethyl Acetate | 5000 | | |\n| Ethyl Ether | 5000 | | |\n| Ethylbenzene | 70 | | |\n\n### Pesticides - CA DCC\n\n| Analyte | Limit (ppb) | Analyte | Limit (ppb) |\n|--------------------|-------------|--------------------|-------------|\n| Acephate | 5000 | Hexythiazox | 2000 |\n| Acetamiprid | 5000 | Imazalil | 30 |\n| Aldicarb | 30 | Imidacloprid | 3000 |\n| Azoxystrobin | 40000 | Kresoxim methyl | 5000 |\n| Bifenazate | 5000 | Malathion | 5000 |\n| Bifenthrin | 5000 | Metalaxyl | 3000 |\n| Boscalid | 1000 | Methiocarb | 30 |\n| Carbaryl | 5000 | Methomyl | 100 |\n| Carbofuran | 30 | Methyl parathion | 30 |\n| Chlorantraniliprole| 40000 | Myclobutanil | 9000 |\n| Chlorfenapyr | 30 | Naled | 500 |\n| Chlorpyrifos | 5000 | Oxamyl | 30 |\n| Clofentezine | 5000 | Paclobutrazol | 30 |\n| Coumaphos | 3000 | Permethrin | 20000 |\n| Cypermethrin | 1000 | Phosmet | 1000 |\n| Daminozide | 30 | Piperonyl Butoxide | 8000 |\n| Diazinon | 30 | Prallethrin | 4000 |\n| Dichlorvos | 30 | Propiconazole | 3000 |\n| Dimethoate | 30 | Propoxur | 30 |\n| Ethoprophos | 30 | Pyrethrins | 3000 |\n| Etofenprox | 3000 | Pyridaben | 3000 |\n| Etoxazole | 1000 | Spinetoram | 12000 |\n| Fenhexamid | 1000 | Spinosad | 12000 |\n| Fenpyroximate | 3000 | Spiromesifen | 12000 |\n| Fipronil | 30 | Spirotetramat | 3000 |\n| Flonicamid | 2000 | Tebuconazole | 3000 |\n| Fludioxonil | 30000 | Thiacloprid | 300 |\n| | | Thiamethoxam | 4500 |\n\n### Mycotoxins - Colorado CDPHE\n\n| Analyte | Limit (ppm) | Analyte | Limit (ppm) |\n|-------------|-------------|-------------|-------------|\n| B1 | 5 | B2 | 5 |\n| G1 | 5 | G2 | 5 |\n| Ochratoxin A| 5 | | |\n\n----\n\nThis product or substance has been tested by KCA Laboratories using validated testing methodologies and an ISO\/IEC 17025:2017 accredited quality system. Values reported relate only to the product or substance tested. The reported result is based on a sample weight. Unless otherwise stated, results of tests performed on all quality control samples met criteria for acceptance established by KCA Laboratories. KCA Laboratories makes no claims as to the efficacy, safety or other risks associated with any detected or non-detected amounts of any substances reported herein. This Certificate of Analysis shall not be reproduced except in full, without the written approval of KCA Laboratories. KCA Laboratories can provide measurement uncertainty upon request."