LabReport (#420)

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# CERTIFICATE OF ANALYSIS

**SAMPLE NAME:** GOLDEN GROVE - PLUM GINGER
**SAMPLE CODE:** DTS-240122-008
**CLIENT:** PICCO BEVERAGES
**BATCH RESULT:** PASS

**MATRIX NAME:** Beverage
**SAMPLE TYPE:** Quality Assurance
**RECEIVED DATE:** Mon, Jan 22, 2024
**PUBLISHED DATE:** Thu, Jan 25, 2024
**BATCH CODE:**
**BATCH SIZE:** 0
**SAMPLE SIZE:** 5U
**AVERAGE UNIT WEIGHT:** 228.65g (1 can)

**TOTAL MAJOR ALKALOIDS:** 38.64 mg/serv
**TOTAL MINOR ALKALOIDS:** ND
**MITRAGYNINE:** 33.84 mg/serv

| ALKU | Kratom Alkaloids<br/>High Level | SAL | Salmonella<br/>GeneUp qPCR 25g | ECOLI | Total E. Coli & Coliforms<br/>Plate | TAMC | Total Aerobic Bacteria<br/>Plate |
| ----- | -------------------------------- | ----- | ------------------------------ | ----- | ------------------------------------ | ----- | ------------------------------------------------ |
| ALKL | Kratom Alkaloids<br/>Low Level | BRX | Brix of Liquids | DEN | Density of Liquids | COOX | Carbon Dioxide &<br/>Dissolved Oxygen of Liquids |
| PH | pH & Electric Conductivity (EC)z | TURB | Turbidity<br/>Liquids | SAUR | Staphylococcus aureus<br/>3M Plating | LMON | Listeria monocytogenes<br/>GeneUp qPCR |
| DIADT | Opioid Adulterants | ENTRO | Enterobacteriaceae<br/>Plate | TMYFD | Total Yeast & Mold<br/>Plate | CAFFE | Caffeine |
| HPMET | Heavy Metals<br/>7 | | | | | | |


----

**RESULTS REVIEWED BY:** Leslie Varela
Laboratory Director
Cambium Analytica
Thursday, Jan 25, 2024

**RESULTS CERTIFIED BY:** Douglas Smith
VP - Scientific Operations
Cambium Analytica
Thu, Jan 25, 2024

*This report may not be reproduced except in full without approval from Cambium Analytica. The results herein relate only to the sample & batch identified in this report.*
---
# DTS-240122-008

## LAB-TM-052 - Determination of Kratom Alkaloid Content by UPLC-DAD
**ALKU-DTS-240122-008-01 - Mon, Jan 22, 2024**

| Analyte | Value | Value (Per Serving) | Value (Per Package) | Action Limit | LOD | LOQ | Status |
|--------------------|--------|---------------------|---------------------|--------------|---------|---------|--------|
| Total Major Alkaloids | 0.017 % | 38.64 mg | 38.64 mg | N/A | 0.3 ug/g | 0.5 ug/g | N/A |
| Mitragynine | 0.015 % | 33.84 mg | 33.84 mg | N/A | 0.3 ug/g | 0.5 ug/g | N/A |
| Paynantheine | 0.001 % | 1.83 mg | 1.83 mg | N/A | 0.3 ug/g | 0.5 ug/g | N/A |
| Speciogynine | 0.001 % | 2.06 mg | 2.06 mg | N/A | 0.3 ug/g | 0.5 ug/g | N/A |
| Speciociliatine | ND | ND | ND | N/A | 0.3 ug/g | 0.5 ug/g | N/A |

## LAB-TM-047 - Determination of Kratom Alkaloid Content by LC-TQ
**ALKU-DTS-240122-008-01 - Mon, Jan 22, 2024**

| Analyte | Value | Value (Per Serving) | Value (Per Package) | Action Limit | LOD | LOQ | Status |
|------------------------|-------|---------------------|---------------------|--------------|-------------|-------------|--------|
| 7-Hydroxymitragynine | ND | ND | ND | N/A | 0.01 ug/kg | 0.1 ug/kg | N/A |
| Total Minor Alkaloids | ND | ND | ND | N/A | 0.01 ug/kg | 0.1 ug/kg | N/A |
| Mitraphylline | ND | ND | ND | N/A | 0.01 ug/kg | 0.1 ug/kg | N/A |

## LAB-TM-063 - Detection and Isolation of Salmonella spp. in Foods and Dietary Supplements
**SAL-DTS-240122-008-01 - Mon, Jan 22, 2024**

| Analyte | Value | Action Limit | LOD | LOQ | Status |
|---------------|-------|--------------|-----|-----|--------|
| Salmonella Spp | ND | N/A | | | N/A |

## LAB-TM-059 - Enumeration of Escherichia Coli and Total Coliform in Foods and Dietary Supplements
**ECOIL-DTS-240122-008-01 - Mon, Jan 22, 2024**

| Analyte | Value | Action Limit | LOD | Status |
|---------------|-----------|--------------|-----|--------|
| E. coli | <10 CFU/g | N/A | | N/A |
| Total Coliforms | <10 CFU/g | N/A | | N/A |

## LAB-TM-060 - Enumeration of Total Aerobic Count in Foods and Dietary Supplements
**TAMC-DTS-240122-008-01 - Mon, Jan 22, 2024**

| Analyte | Value | Action Limit | LOD | LOQ | Status |
|--------------------|-----------|--------------|-----|-----|--------|
| Total Aerobic Count | <10 CFU/g | N/A | | | N/A |

## LAB-TM-017 - Brix & Density Analysis
**BRX-DTS-240122-008-01 - Mon, Jan 22, 2024**

| Analyte | Value | Action Limit | LOD | LOQ | Status |
|---------|--------|--------------|-----|-----|--------|
| Brix | 10.9 bx | N/A | | | N/A |

## LAB-TM-017 - Brix & Density Analysis
**DEN-DTS-240122-008-01 - Mon, Jan 22, 2024**

| Analyte | Value | Action Limit | LOD | LOQ | Status |
|---------|---------|--------------|-----|-----|--------|
| Density | 1.042 g/mL | N/A | | | N/A |

## LAB-TM-020 - Determination of Carbon Dioxide and Dissolved Oxygen in Beverages
**COOX-DTS-240122-008-01 - Mon, Jan 22, 2024**

| Analyte | Value | Action Limit | LOD | LOQ | Status |
|-----------------------|-----------|--------------|-----|-----|--------|
| Dissolved Carbon Dioxide | 1.72 vol | N/A | | | N/A |
| Dissolved Oxygen | 40.35 ug/kg | N/A | | | N/A |

---
# DTS-240122-008

## LAB-TM-018 - Test Method for Determining pH
**PH-DTS-240122-008-01 - Mon, Jan 22, 2024**

| Analyte | Value | Action Limit | LOD | LOQ | Status |
|---------|-------|--------------|-----|-----|--------|
| pH | 3.401 | N/A | N/A | N/A | N/A |

## LAB-TM-021 - Turbidity by UV-VIS
**TURB-DTS-240122-008-01 - Mon, Jan 22, 2024**

| Analyte | Value | Action Limit | LOD | LOQ | Status |
|-----------|----------|--------------|-----|-----|--------|
| Turbidity | 71.307 % | N/A | N/A | N/A | N/A |

## LAB-TM-062 - Enumeration of Staphylococcus aureus in Foods and Dietary Supplements
**SAUR-DTS-240122-008-01 - Mon, Jan 22, 2024**

| Analyte | Value | Action Limit | LOD | LOQ | Status |
|-----------|-----------|--------------|-----|-----|--------|
| S. aureus | <10 CFU/g | N/A | N/A | N/A | N/A |

## LAB-TM-064 - Detection and Isolation of L. monocytogenes in Foods and Dietary Supplements
**LMON-DTS-240122-008-01 - Mon, Jan 22, 2024**

| Analyte | Value | Action Limit | LOD | LOQ | Status |
|-----------------------|-------|--------------|-----|-----|--------|
| Listeria monocytogenes | ND | N/A | N/A | N/A | N/A |

## LAB-TM-074 - Qualitative Determination of Pain Management Adulterants in Botanical Products
**DTADT-DTS-240122-008-01 - Mon, Jan 22, 2024**

| Analyte | Value | Action Limit | LOD | LOQ | Status |
|--------------------------|-------|--------------|-----------|-----|--------|
| 4-Fluoro-Isobutyryl Fentanyl | ND | Detection | 1.20 ug/g | | PASS |
| Acetyl Fentanyl | ND | Detection | 0.48 ug/g | | PASS |
| Benzoyl Fentanyl | ND | Detection | 0.48 ug/g | | PASS |
| Buprenorphine | ND | Detection | 4.80 ug/g | | PASS |
| Butyryl Fentanyl | ND | Detection | 1.20 ug/g | | PASS |
| Carfentanyl | ND | Detection | 1.20 ug/g | | PASS |
| Codeine | ND | Detection | 4.80 ug/g | | PASS |
| Cyclopropyl Fentanyl | ND | Detection | 0.48 ug/g | | PASS |
| Fentanyl | ND | Detection | 0.48 ug/g | | PASS |
| Furanyl Fentanyl | ND | Detection | 0.48 ug/g | | PASS |
| Heroin | ND | Detection | 4.80 ug/g | | PASS |
| Hydrocodone | ND | Detection | 4.80 ug/g | | PASS |
| Hydromorphone | ND | Detection | 4.80 ug/g | | PASS |
| Meperidine | ND | Detection | 4.80 ug/g | | PASS |
| Methadone | ND | Detection | 4.80 ug/g | | PASS |
| Morphine | ND | Detection | 4.80 ug/g | | PASS |
| Oxycodone | ND | Detection | 4.80 ug/g | | PASS |
| Oxymorphone | ND | Detection | 4.80 ug/g | | PASS |
| Tramadol | ND | Detection | 4.80 ug/g | | PASS |

---
# DTS-240122-008

## LAB-TM-084 - ENUMERATION OF ENTEROBACTERIACEAE
**ENTRO-DTS-240122-008-01 - MON, JAN 22, 2024**

| Analyte | Value | Action Limit | LOD | LOQ | Status |
|--------------------|-------------|--------------|-----------|-----------|--------|
| Enterobacteriaceae | <10 CFU/g | N/A | 100 CFU/g | 100 CFU/g | N/A |

## LAB-TM-061 - ENUMERATION OF YEAST AND MOLD IN FOODS AND DIETARY SUPPLEMENTS
**TYMFD-DTS-240122-008-01 - MON, JAN 22, 2024**

| Analyte | Value | Action Limit | LOD | LOQ | Status |
|-------------------|-----------|--------------|-----------|-----------|--------|
| Total Yeast and Mold | <10 CFU/g | N/A | N/A | N/A | N/A |

## LAB-TM-076 - DETERMINATION OF CAFFEINE AND MELATONIN BY HPLC
**CAFFE-DTS-240122-008-01 - MON, JAN 22, 2024**

| Analyte | Value (Per Serving) | Value (Per Package) | Action Limit | LOD | LOQ | Status |
|----------|---------------------|---------------------|--------------|-----------|-----------|--------|
| Caffeine | 0.0531 mg/g | 12.13 mg | N/A | 0.025 mg/g | 0.05 mg/g | N/A |

## LAB-TM-044 - DETERMINATION OF HEAVY METALS BY ICP-MS
**HPMET-DTS-240122-008-01 - MON, JAN 22, 2024**

| Analyte | Value | Action Limit | LOD | LOQ | Status |
|----------|--------|--------------|-------------|-------------|--------|
| Arsenic | ND | N/A | 0.1985 ug/kg | 0.6616 ug/kg | N/A |
| Cadmium | ND | N/A | 0.0817 ug/kg | 0.2724 ug/kg | N/A |
| Chromium | 0.012 ug/g | N/A | 0.6272 ug/kg | 2.0907 ug/kg | N/A |
| Copper | ND | N/A | 0.1546 ug/kg | 0.5152 ug/kg | N/A |
| Lead | 0.005 ug/g | N/A | 0.2817 ug/kg | 0.2817 ug/kg | N/A |
| Mercury | ND | N/A | 0.0171 ug/kg | 0.0571 ug/kg | N/A |
| Nickel | 0.007 ug/g | N/A | 0.3213 ug/kg | 1.0709 ug/kg | N/A |